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Screening of textile finishing agents available on the Chinese market: An important source of per- and

Mehvish Mumtaz, Yixiang Bao, Wenchao Li, Lingxiao Kong, Jun Huang, Gang Yu

《环境科学与工程前沿（英文）》 2019年第13卷第5期 doi: 10.1007/s11783-019-1145-0

摘要： Kendrick mass defect was used for PFASs screening in textile finishing agents (TFAs). Total oxidizable precursor assay provides insight into unknown precursors. Perfluorooctane sulfonate was found as impurity in short ECF technology based TFAs. Perfluorooctanoate was also detected in C6 telomerization based TFAs. Long chain precursors were also observed in both types of TFAs. Organofluorinated surfactants are widely employed in textile finishing agents (TFAs) to achieve oil, water, and stain repellency. This has been regarded as an important emission source of per-and polyfluoroalkyl substances (PFASs) to the environment. China is the biggest manufacturer of clothes, and thus TFA production is also a relevant industrial activity. Nevertheless, to date, no survey has been conducted on PFAS contents in commercially available TFAs. In the present study, TFA products were investigated by the Kendrick mass defect method. The quantification results demonstrated a significant presence of perfluorooctane sulfonate (0.37 mg/L) in TFAs manufactured by electrochemical fluorination technology. The products obtained by short-chain PFAS-based telomerization were dominated by perfluorooctanoic acid (mean concentration: 0.29 mg/L), whose values exceeded the limits stated in the European Chemical Agency guidelines (0.025 mg/L). Moreover, the total oxidizable precursor assay indicated high levels of indirectly quantified precursors with long alkyl chains (C7–C9). Together, these results suggest that there is currently a certain of environmental and health risks in China that originates from the utilization of TFAs, and a better manufacturing processes are required to reduce such risks.

关键词： Textile finishing agents Kendrick mass defect Total oxidizable precursor assay

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让人们穿得更好——21世纪纺织科学与工程学科的前沿概述

姚穆

《中国工程科学》 2003年第5卷第4期页码 47-49

摘要：

“纺织科学与工程”学科多年来有了很大发展，中国人民告别了缺吃少穿的历史。纺织品和服装在我国的国民经济中占相当重要的地位，出口创汇和顺差占显著的位置。为了迎接新世纪的挑战，21世纪的纺织科学与工程学科的前沿将主要围绕着发展开发新品种，实现新功能；引进高新科学技术，加速改造纺织科学与工程学科；新型纺织染整加工新技术与设备的发展；纺织生产、经营、销售、交付、运输、资金等新的管理运转模式的转变等四个方面。21世纪将是产业用纺织品飞速发展的时代。

关键词： “纺织科学与工程”学科智能服装产业用纺织品纺织纤维纺、织、染整

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Experimental investigation on concrete overlaid with textile reinforced mortar: Influences of mix, temperature

《结构与土木工程前沿（英文）》 2023年第17卷第2期页码 271-283 doi: 10.1007/s11709-022-0896-z

摘要： Textile reinforced mortar is widely used as an overlay for the repair, rehabilitation, and retrofitting of concrete structures. Recently, textile reinforced concrete has been identified as a suitable lining material for improving the durability of existing concrete structures. In this study, we developed a textile-reinforced mortar mix using river sand and evaluated the different characteristics of the textile-reinforced mortar under various exposure conditions. Studies were carried out in two phases. In the first phase, the pullout strength, temperature resistance, water absorption, and compressive and bending strength values of three different textile-reinforced mortar mixes with a single type of textile reinforcement were investigated. In the second phase, the chemical resistance of the mix that showed the best performance in the abovementioned tests was examined for use as an overlay for a concrete substrate. Investigations were performed on three different thicknesses of the textile reinforced mortar overlaid on concrete specimens that were subjected to acidic and alkaline environments. The flexural responses and degradations of the textile reinforced mortar overlaid specimens were examined by performing bending tests. The experimental findings indicated the feasibility of using textile reinforced mortar as an overlay for durable concrete construction practices.

关键词： textile reinforced mortar bending tests acid and alkaline environment concrete overlay

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Numerical modelling of reinforced concrete flexural members strengthened using textile reinforced mortars

《结构与土木工程前沿（英文）》 2023年第17卷第4期页码 649-668 doi: 10.1007/s11709-023-0919-4

摘要： Externally bonded (EB) and near-surface mounted (NSM) bonding are two widely adopted and researched strengthening methods for reinforced-concrete structures. EB composite substrates are easy to reach and repair using appropriate surface treatments, whereas NSM techniques can be easily applied to the soffit and concrete member sides. The EB bonded fiber-reinforced polymer (FRP) technique has a significant drawback: combustibility, which calls for external protective agents, and textile reinforced mortar (TRM), a class of EB composites that is non-combustible and provides a similar functionality to any EB FRP-strengthened substrate. This study employs a finite element analysis technique to investigate the failing failure of carbon textile reinforced mortar (CTRM)-strengthened reinforced concrete beams. The principal objective of this numerical study was to develop a finite element model and validate a set of experimental data in existing literature. A set of seven beams was modelled and calibrated to obtain concrete damage plasticity (CDP) parameters. The predicted results, which were in the form of load versus deflection, load versus rebar strain, tensile damage, and compressive damage patterns, were in good agreement with the experimental data. Moreover, a parametric study was conducted to verify the applicability of the numerical model and study various influencing factors such as the concrete strength, internal reinforcement, textile roving spacing, and externally-applied load span. The ultimate load and deflection of the predicted finite element results had a coefficient of variation (COV) of 6.02% and 5.7%, respectively. A strain-based numerical comparison with known methods was then conducted to investigate the debonding mechanism. The developed finite element model can be applied and tailored further to explore similar TRM-strengthened beams undergoing debonding, and the preventive measures can be sought to avoid premature debonding.

关键词： fiber reinforced polymer textile reinforced mortar finite element analysis concrete damage plasticity calibration and validation parametric study

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2017年度环境与轻纺工程前沿

环境与轻纺工程项目组

《全球工程前沿》 2017年第1卷第1期页码 152-178

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Adsorption in combination with ozonation for the treatment of textile waste water: a critical review

Shraddha Khamparia,Dipika Kaur Jaspal

《环境科学与工程前沿（英文）》 2017年第11卷第1期 doi: 10.1007/s11783-017-0899-5

摘要： A combination of adsorption with ozonation proved best for dye removal. Toxicity of the textile effluents can be remarkably reduced by combined method. Wide scope for choice of natural materials for treatment of textile dyes. Intrusion of synthetic textile dyes in the ecosystem has been recognized as a serious issue worldwide. The effluents generated from textiles contain large amount of recalcitrant unfixed dyes which are regarded as emerging contaminants in the field of waste water study. Removal of various toxic dyes often includes diverse and complex set of physico-chemical, biological and advanced oxidation processes adopted for treatment. Adsorption in itself is a well-known technique utilized for treatment of textile effluents using a variety of adsorbents. In addition, ozonation deals with effective removal of dyes using high oxidising power of ozone. The review summarizes dye removal study by a combination of ozonation and adsorption methods. Also, to acquire an effective interpretation of this combined approach of treating wastewater, a thorough study has been made which is deliberated here. Results asserts that, with the combined ability of ozone and a catalyst/adsorbent, there is high possibility of total elimination of dyes from waste water. Several synthetically prepared materials have been used along with few natural materials during the combined treatment. However, considering practical applicability, some areas were identified during the study where work needs to be done for effective implementation of the combined treatment.

关键词： Adsorption Ozonation Catalytic Ozonation Textile dyes Mineralization

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Sub-nanometer finishing of polycrystalline tin by inductively coupled plasma-assisted cutting

《机械工程前沿（英文）》 2023年第18卷第3期 doi: 10.1007/s11465-023-0751-5

摘要： Polycrystalline tin is an ideal excitation material for extreme ultraviolet light sources. However, the existence of grain boundary (GB) limits the surface roughness of polycrystalline tin after single-point diamond turning (SPDT). In this work, a novel method termed inductively coupled plasma (ICP)-assisted cutting was developed for the sub-nanometer finishing of polycrystalline tin. The relationship between ICP power, processing time, and modification depth was established by thermodynamic simulation, and the fitted heat transfer coefficient of polycrystalline tin was 540 W/(m²·K). The effects of large-thermal-gradient ICP treatment on the microstructure of polycrystalline tin were studied. After 0.9 kW ICP processing for 3.0 s, corresponding to the temperature gradient of 0.30 K/µm, the grain size of polycrystalline tin was expanded from a size of approximately 20–80 μm to a millimeter scale. The Taguchi method was used to investigate the effects of rotational speed, depth of cut, and feed rate on SPDT. Experiments conducted based on the ICP system indicated that the plasma-assisted cutting method promoted the reduction of the influence of GB steps on the finishing of polycrystalline tin, thereby achieving a surface finish from 8.53 to 0.80 nm in Sa. The results of residual stress release demonstrated that the residual stress of plasma-assisted turning processing after 504 h stress release was 10.7 MPa, while that of the turning process without the ICP treatment was 41.6 MPa.

关键词： plasma-assisted cutting polycrystalline tin single-point diamond turning surface roughness

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Evaluation of 1,4-naphthoquinone derivatives as antibacterial agents: activity and mechanistic studies

《环境科学与工程前沿（英文）》 2023年第17卷第3期 doi: 10.1007/s11783-023-1631-2

摘要：

● All 1,4-naphthoquinone hybrids exhibited significant antimicrobial activity.

关键词： 1 4-naphthoquinone derivatives Antibacterial Action mechanism RecA

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2018年度环境与轻纺工程前沿

环境与轻纺工程项目组

《全球工程前沿》 2018年第2卷第1期页码 140-163

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2023年度环境与轻纺工程前沿

环境与轻纺工程项目组

《全球工程前沿》 2023年第7卷第1期页码 156-180

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Novel lysosome-targeted anticancer fluorescent agents used in zebrafish and nude mouse tumour imaging

《化学科学与工程前沿（英文）》 2022年第16卷第1期页码 112-120 doi: 10.1007/s11705-021-2075-5

摘要： The design of three novel fatty nitrogen mustard-based anticancer agents with fluorophores incorporated into the alkene structure (CXL 118, CXL121, and CXL122) is described in this report. The results indicated that these compounds are selectively located in lysosomes and exhibit effective antitumour activity. Notably, these compounds can directly serve as both reporting and imaging agents in vitro and in vivo without the need to add other fluorescent tagging agents.

关键词： fluorescent drug lysosomal anticancer zebrafish nude-mouse tumour imaging

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Comparison of masking agents for antimony speciation analysis using hydride generation atomic fluorescence

Jianhong XI,Mengchang HE,Kunpeng WANG,Guizhi ZHANG

《环境科学与工程前沿（英文）》 2015年第9卷第6期页码 970-978 doi: 10.1007/s11783-014-0716-3

摘要： A sensitive atomic spectrometric method for the redox speciation analysis of Sb in water is described. The proposed method is based on the selective generation of stibine from Sb(III) in a continuous flow system using non-dispersive atomic fluorescence spectrometry for detection. The effects of the HCl concentration on the fluorescence intensities of Sb(III) and Sb(V) were investigated. The results indicated that atomic fluorescence emission due to Sb(V) can constructively interfere with the determination of Sb(III). For the determination of Sb(III), four compounds were tested as masking agents to inhibit the generation of stibine from Sb(V). The effects of the concentrations of the masking agents and of HCl on the fluorescence signals from Sb(III) and Sb(V) were studied. The results indicated that citric acid and NaF can successfully suppress hydride generation from Sb(V). To evaluate the developed methodology and the influence of the matrix, the recovery of Sb(III) from natural water that was spiked with different Sb(III) and Sb(V) concentrations was tested.

关键词： Sb(III) Sb(V) determination masking agents hydride generation (HG-AFS)